A combination of finite element analysis (FEA) calculations and resonant frequency measurements are applied for determining normal and lateral spring constants of microfabricated ceramic/gold cantilevers for friction force microscopes. The cantilever Si3N4 and Au layers are combined analytically into an equivalent single composite layer. Bending and torsion behavior of the cantilever under typical operating forces are determined through FEA. Effective Young’s modulus for the composite Si3N4-Au beam from 172 to 185 GPa is determined through assimilation of FEA and fundamental resonant frequency measurements. Several current analytical solutions are compared to the full FEA evaluation. A new analytical expression is derived for obtaining the ratio of lateral to normal spring constants and thereby evaluation of absolute values of friction coefficients. Calibration plots are presented for assessment of both vertical and torsion spring constants of bicomponent cantilevers by measuring their resonant frequencies and thickness of gold overlay.

1.
Albrecht
T. R.
,
Akamine
S.
,
Carver
T. E.
, and
Quale
C. F.
,
1990
, “
Microfabrication of Cantilever Styli for the Atomic Force Microscope
,”
J. Vac. Sci. and Technol.
, Vol.
A8
, pp.
3386
3396
.
2.
Beer, F. P., and Johnson Jr., E. R., 1981, Mechanics of Materials, McGraw-Hill, NY.
3.
Bhushan
B.
, and
Blackman
G. S.
,
1991
, “
Atomic Force Microscopy of Magnetic Rigid Discs and Sliders and Its Application to Tribology
,”
ASME JOURNAL OF TRIBOLOGY
, Vol.
113
, pp.
452
457
.
4.
Bhushan
B.
, and
Ruan
J.-A.
,
1994
, “
Atomic Scale Friction Measurements Using Friction Force Microscopy: II
,”
ASME JOURNAL OF TRIBOLOGY
, Vol.
116
, pp.
389
396
.
5.
Bhushan
B.
,
Israelachvili
J. N.
, and
Landman
U.
,
1995
, “
Nanotribology; Friction, Wear, and Lubrication at the Atomic Scale
,”
Nature
, Vol.
374
, pp.
607
616
.
6.
Bhushan
B.
,
Kulkarni
A. V.
,
Koinkar
V. N.
,
Boehm
M.
,
Odoni
L.
,
Martelet
C.
, and
Belin
M.
,
1995
, “
Microtribological Characterization of Self-Assembled and Langmuir-Blodgett Monolayers by Atomic and Friction Force Microscopy
,”
Langmuir
, Vol.
11
, pp.
3189
3198
.
7.
Bliznyuk, V. N., Everson, M. P., and Tsukruk, V. V., 1998, “Nanotribological Properties of Organic Boundary Lubricants; Langmuir Films Versus Self-Assembled Monolayers,” ASME JOURNAL OF TRIBOLOGY, accepted for publication.
8.
Burnham
N. A.
,
Dominquez
D.
,
Mowery
R. L.
, and
Colton
R. J.
,
1990
, “
Probing of Surface Forces of Monolayer Films with an Atomic-Force Microscope
,”
Phys. Rev. Lett.
, Vol.
64
, pp.
1931
1934
.
9.
Butt
H.-J.
,
Siedle
P.
,
Seifert
K.
,
Fendler
K.
,
Seeger
T.
,
Bamberg
E.
,
Weise-nhorn
A. L.
,
Goldie
K.
, and
Engel
A.
,
1993
, “
Scan Speed Limit in Atomic Force Microscopy
,”
J. Microscopy
, Vol.
169
, pp.
75
84
.
10.
Cleveland
J.
,
Manne
S.
,
Bocek
D.
, and
Hansma
P. K.
,
1993
, “
A Nondestructive Method for Determining the Spring Constant of Cantilevers for Scanning Force Microscopy
,”
Rev. Sci. Instrum.
, Vol.
64
, pp.
403
405
.
11.
Cleveland, J., 1996, “Spring Constant Update,” unpublished results. Digital Instruments, Santa Barbara, CA.
12.
Cutiongo
B. C.
,
Li
D.
,
Chung
Y.
, and
Bhatia
C. S.
,
1996
, “
Tribological Behavior of Amorphous Carbon Nitride Overcoats for Magnetic Discs
,”
ASME JOURNAL OF TRIBOLOGY
, Vol.
118
, pp.
543
549
.
13.
Friedenberg
M. C.
, and
Mate
C. M.
,
1996
, “
Dynamic Viscoelastic Properties of Liquid Polymer Films Studied by Atomic Force Microscopy
,”
Langmuir
, Vol.
12
, pp.
6138
6142
.
14.
Green
J.-B.
,
McDermot
M. T.
,
Porter
M. D.
, and
Siperko
L. M.
,
1995
, “
Nanometer-Scale Mapping of Chemically Distinct Domains Using Frictional Force Microscopy
,”
J. Phys. Chem.
, Vol.
99
, pp.
10960
10965
.
15.
Hazel
J.
, and
Tsukruk
V. V.
,
1996
, “
Quantitative Force Measurements in • SPM; Vertical and Torsional Spring Constants for V-shaped Cantilevers
,”
Polymer Prepr.
, Vol.
37
(
2
), pp.
567
568
.
16.
Hazel, J., and Tsukruk, V. V., 1998, “Spring Constants Of Microfabricated Ceramic/Gold Cantilevers For Scanning Probe Microscopy,” Thin Solid Films, accepted.
17.
Jiang
Z.
,
Lu
C-J.
,
Bogy
D. B.
, and
Miyamoto
T.
,
1995
, “
Dependence of Nano-Friction and Nano-Wear on Loading Force for Sharp Diamond Tips Sliding on Si, Mn-Zn Ferrite, and Au
,”
ASME JOURNAL OF TRIBOLOGY
, Vol.
117
, pp.
328
341
.
18.
Elliot, D., 1986, Microlithography: Process Technology for IC Fabrication, Halliday Lith., NY.
19.
Labardi
M.
,
Allegrini
M.
,
Salerno
M.
,
Frediani
C.
, and
Ascoli
C.
,
1994
, “
Dynamical Friction Coefficient Map Using a Scanning Force and Friction Microscope
,”
Appl. Phys.
,
A74
, pp.
3
10
.
20.
Mate
C. M.
,
McClelland
G. M.
,
Erlandsson
R.
, and
Chiang
S.
,
1987
, “
Atomic-Scale Friction of a Tungsten Tip on a Graphite Surface
,”
Phys. Rev. Lett.
, Vol.
59
, pp.
1942
1945
.
21.
Meyer
E.
,
Overney
R.
,
Luthi
R.
,
Brodbeck
D.
,
Howard
L.
,
Frommer
J.
,
Guntherodt
H-J.
,
Wolter
O.
,
Fujihira
M.
,
Takano
T.
, and
Gotoh
Y.
,
1992
, “
Friction Force Microscopy of Mixed Langmuir-Blodgett Films
,”
Thin Solid Films
, Vol.
220
, pp.
132
137
.
22.
Neumeister
J. M.
, and
Ducker
W. A.
,
1994
, “
Lateral, Normal, and Longitudinal Spring Constants of Atomic Force Microscopy Cantilevers
,”
Rev. Sci. Instrum.
, Vol.
65
, pp.
2527
2531
.
23.
Noy
A.
,
Frisbie
C. D.
,
Rozsnyai
L. F.
,
Wrighton
M. S.
, and
Lieber
C. M.
,
1995
, “
Chemical Force Microscopy: Exploiting Chemically-Modified Tips to Quantify Adhesion, Friction, and Functional Group Distribution in Molecular Assemblies
,”
J. Am. Chem. Soc
, Vol.
117
, pp.
7943
7951
.
24.
Ogletree
D. F.
,
Carpick
R. W.
, and
Salmeron
M.
,
1996
, “
Calibration of Frictional Forces in Atomic Force Microscopy
,”
Rev. Sci. Instrum.
, Vol.
67
, pp.
3298
3305
.
25.
Overney
R.
,
Meyer
E.
,
Frommer
J.
,
Brodbeck
D.
,
Luthi
R.
,
Howard
L.
,
Guntherodt
H-J.
,
Wolter
O.
,
Fujihira
M.
,
Takano
T.
, and
Gotoh
Y.
,
1992
, “
Friction Measurements on Phase-Separated Thin Films with A Modified Atomic Force Microscopy
,”
Nature
, Vol.
359
, pp.
133
135
.
26.
Overney
R. M.
,
1995
, “
Nanotribological Studies of Polymers
,”
Trends in Palym. Sci.
, Vol.
3
, pp.
359
364
.
27.
Peterson
K. E.
, and
Guarnieri
C. R.
,
1979
, “
Young’s Modulus Measurements of Thin Films Using Micromechanics
,”
J. Appl. Phys.
, Vol.
50
, pp.
6761
6766
.
28.
Ruan
J.-A.
, and
Bhushan
B.
,
1994
, “
Atomic Scale Friction Measurements Using Friction Force Microscopy: I
,”
ASME JOURNAL OF TRIBOLOGY
, Vol.
116
, pp.
378
388
.
29.
Sader
J. E.
,
1995
, “
Parallel Beam Approximation for V-shaped Atomic Force Microscope Cantilevers
,”
Rev. Sci. Instrum.
, Vol.
66
, pp.
4583
4587
.
30.
Sader
J. E.
,
Larson
I.
,
Mulvaney
P.
, and
White
L. R.
,
1995
, “
Method for the Calibration of Atomic Force Microscope Cantilevers
,”
Rev. Sci. Instrum.
, Vol.
66
, pp.
3789
3798
.
31.
Senden
T.
, and
Ducker
W.
,
1994
, “
Experimental Determination of Spring Constants in Atomic Force Microscopy
,”
Langmuir
, Vol.
10
, pp.
1003
1004
.
32.
Tsukruk
V. V.
,
Bliznyuk
V. N.
,
Hazel
J.
,
Visser
D.
, and
Everson
M. P.
,
1996
a, “
Organic Molecular Films Under Shear Forces; Fluid and Solid Langmuir Monolayers
,”
Langmuir
, Vol.
12
, pp.
4840
4849
.
33.
Tsukruk
V. V.
,
Everson
M. P.
,
Lander
L. M.
, and
Brittain
W. J.
,
1996
b, “
Nanotribological Properties of Composite Molecular Films: C60 Anchored to a Self-Assembled Monolayer
,”
Langmuir
, Vol.
12
, pp.
3905
3913
.
34.
Tsukruk
V. V.
,
Bliznyuk
V. N.
,
Visser
D.
, and
Hazel
J.
,
1996
c, “
Reconstruction of Fluid Langmuir Monolayers under Shear Forces
,”
Tribology Letter.
, Vol.
2
, pp.
71
77
.
35.
Tsukruk
V. V.
,
Bliznyuk
V. N.
, and
Everson
M. P.
,
1996
d, “
Nanotribology of Composite Molecular Layers
,”
Polymer Prepr.
, Vol.
37
(
2
), pp.
557
558
.
36.
Tsukruk, V. V., and Ratner, B., Eds., 1998, Scanning Probe Microscopy in Polymers, ACS Symposium Series, Washington DC, v. 694.
37.
Tsukruk
V. V.
,
1998
a, “
Scanning Probe Microscopy of Polymer Surfaces
,”
Rubber Chem. Techn.
, Vol.
70
, pp.
432
480
.
38.
Tsukruk
V. V.
, and
Bliznyuk
V. N.
,
1998
b, “
Adhesive and friction forces probed by chemically modified SPM tips
,”
Langmuir
, Vol.
14
, pp.
446
455
.
39.
Walters
D. A.
,
Cleveland
J. P.
,
Thomson
N. H.
,
Hansma
P. K.
,
Wendman
M. A.
,
Gurdey
G.
, and
Ellings
V.
,
1996
, “
Short Cantilevers for Atomic Force Microscopy
,”
Rev. Sci. Instrum.
, Vol.
67
, pp.
3583
3590
.
40.
Warmack
R. J.
,
Zheng
X.-Y.
,
Thundat
T.
, and
Allison
D. P.
,
1994
, “
Friction Effects in the deflection of Atomic Force Microscope Cantilevers
,”
Rev. Sci. Instrum.
, Vol.
65
, pp.
394
399
.
This content is only available via PDF.
You do not currently have access to this content.